ISSN print edition: 0366-6352
ISSN electronic edition: 1336-9075
Registr. No.: MK SR 9/7
Solid-state vibrational spectra and theoretical study of alaninamide acetate
Institute of Organic Chemistry, Bulgarian Academy of Sciences, Acad. G. Bonchev Str. 9, 1113 Sofia, Bulgaria
Received: 26 April 2007 Revised: 6 June 2007 Accepted: 7 June 2007
Abstract: Solid-state IR and Raman spectroscopic elucidation of alaninamide acetate is preformed by means of the possibilities of linear-polarized
IR and Raman methods. The experimental assignment is compared with theoretical vibrational analysis with the intention to
explain the influence of intermolecular interactions in solid phase on the spectroscopic properties of the compound studied.
The 1H and 13C NMR spectra in solution are compared with the corresponding ones of alanine, studying the amidation effect on the chemical
shift signals in the alanine moieties.
Keywords: alaninamide acetate - IR and Raman spectroscopy - solid state - IR-LD study - vibrational analysis -
1H and 13C NMR
Full paper is available at www.springerlink.com.
Chemical Papers 61 (6) 502–506 (2007)
Wednesday, September 28, 2022