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Solid-state vibrational spectra and theoretical study of alaninamide acetate

T. Kolev

Institute of Organic Chemistry, Bulgarian Academy of Sciences, Acad. G. Bonchev Str. 9, 1113 Sofia, Bulgaria

 

E-mail: kolev@orgchm.bas.bg

Received: 26 April 2007  Revised: 6 June 2007  Accepted: 7 June 2007

Abstract: Solid-state IR and Raman spectroscopic elucidation of alaninamide acetate is preformed by means of the possibilities of linear-polarized IR and Raman methods. The experimental assignment is compared with theoretical vibrational analysis with the intention to explain the influence of intermolecular interactions in solid phase on the spectroscopic properties of the compound studied. The 1H and 13C NMR spectra in solution are compared with the corresponding ones of alanine, studying the amidation effect on the chemical shift signals in the alanine moieties.

Keywords: alaninamide acetate - IR and Raman spectroscopy - solid state - IR-LD study - vibrational analysis -  1H and 13C NMR

Full paper is available at www.springerlink.com.

DOI: 10.2478/s11696-007-0069-5

 

Chemical Papers 61 (6) 502–506 (2007)

Wednesday, September 28, 2022

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