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5,6-Unsaturated amylose derivatives

Š. Bauer and K. Tihlárik

Chem. Inst., Slovak Acad. Sci., Bratislava

 

Abstract:  By the direct halogenation of 2,3-di-O-acetyIamylose with triphenylphosphine and N-iodosuccinimide was prepared 2,3-di-O-acetyl-6-iodo-6-deoxyamylose. The degree of substitution (iodine) was 0.50. Elimination of hydrogen iodide in methanolic solution -of potassium hydroxide afforded 5,6-amylosene contai ing 41.10% of 6-deoxy-glucose-5,6-en units.

Full paper in Portable Document Format: 302a223.pdf (in German)

 

Chemical Papers 30 (2) 223–225 (1976)

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