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Synthesis and biological activity of O,O-dialkyl S-(5-phenyl-5,6-dihydro-1,4-dithiin-2,3-dicarboximidomethyl) thio- and dithiophosphates

F. Gregáň, V. Konečný, Ľ. Jozefíni, and A. Nagy

Department of Inorganic and Organic Chemistry, Faculty of Pharmacy, Komenský University, SSO 34 Bratislava

 

Abstract: 0,0-Dialkyl 5-(5-phenyl-5,6-dihydro-1,4-dithiin-2,3-dicarboximidomethyl) thiophosphates and 0,0-dialkyl 5-(5-phenyl-5,6-dihydro-1,4-dithiin-2,3-dicarboximidomethyl) dithiophosphates were prepared from N-chloromethyl-5-phenyl-5,6-dihydro-1,4-dithiin-2,3-dicarboximide and potassium salts of 0,0-dialkyl thiophosphoric and 0,0-dialkyl dithiophosphoric acids. Electronic and infrared spectra of all the prepared compounds and in the case of compounds III, IV, and IX also 1H-NMR spectra were interpreted.

Full paper in Portable Document Format: 304a547.pdf

 

Chemical Papers 30 (4) 547–552 (1976)

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