ISSN print edition: 0366-6352 ISSN electronic edition: 1336-9075 Registr. No.: MK SR 9/7 Published monthly

Isothiocyanates and Their Synthetic Producers. XII. Preparation of 3,5-Disubstituted Tetrahydro-1,3,5-thiadiazine-2-thiones Labeled with ¹⁴C and ³⁵S

J. Augustín, J. Bernát, Ľ. Drobnica, and P. Kristián

Department of Microbiology and Biochemistry, Slovak Technical University, Bratislava 1

Abstract:  The preparation of 3,5-dibenzyltetrahydro-l,3,5-thiadiazine-2-thione-³⁵S by isotopic substitution with ³⁵S is described. Also the preparation of 3-(4-bromophenyl)-5-benzyltetrahydro-l,3,5-thiadiazine-2-thione-³⁵S from 4-bromophenyl isothiocyanate-³⁵S and of 3-benzyl-5-carboxymethyltetrahydro-1,3,5-thiadiazine-2-thione-¹⁴C from glycine-¹⁴C is described.

Full paper in Portable Document Format: 254a304.pdf

Chemical Papers 25 (4) 304–307 (1971)