ISSN print edition: 0366-6352 ISSN electronic edition: 1336-9075 Registr. No.: MK SR 9/7 Published monthly

Gas chromatography of trimethylsilyl ethers of some 17-oxo steroids

D. Podhradský and M. Š. Kandráč

Research Laboratory, Department of Internal Medicine, Medical Faculty, University of P. J, Šafárik, Košice

Abstract: Trimethylsilyl ethers of 17-ketosteroids were separated by gas chromatography through the use of NGS, and QF-1 phases. Relative retention times found in the mentioned phases with innert supports Chromosorb W, and Gas Chrom Q are compared. Advantages, and an availability of described phases for the separation of 17-ketosteroids occuring in human urine are discussed.

Full paper in Portable Document Format: 233a224.pdf

Chemical Papers 23 (3) 224–228 (1969)