ISSN print edition: 0366-6352 ISSN electronic edition: 1336-9075 Registr. No.: MK SR 9/7 Published monthly

The reaction of N-chlorosuccinimide with O,O-dialkyldithiophosphoric acids

Š. Truchlík, J. Mašek, and J. Drábek

Forschungsinstitut für agrochemische Technologie in Bratislava-Predmestie

Abstract: By reaction of O,O-dialkyldithiophosphoric acids, HCl, and N-chlorosuccinimide the following bis(O,O-dialkylthiophosphoryl) disulfides were prepd.: [(EtO)₂.PS₂]₂, b1-2 170-8° Pr analog, b1 23-4°, d20 1.1676, n20D 1.5392; iso-Pr analog, b. 91-3° Bu analog, d20 1.1205, n20D 1.5309; iso-Bu analog, d20 1.1110, n20D 1.5242; cyclohexyl analog, b. 77-8.5°.

Full paper in Portable Document Format: 1110a579.pdf (in Slovak)

Chemical Papers 11 (10) 579–582 (1957)